Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Base Information

Chemical Name:Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester
CAS No.:215321-43-0
Molecular Formula:C₁₈H₂₃ClO₃
Molecular Weight:322.832
Hs Code.:

Synonyms:Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Chemical Property of Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

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Technology Process of Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

There total 1 articles about Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79-37-8
oxalyl dichloride

: 65253-04-5
(-)-8-phenylmenthol

: 215321-43-0
Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

Guidance literature:: In chloroform; for 2h; Ambient temperature;
DOI:10.1055/s-1998-2198

Reference yield:

: 215321-43-0
Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 84312-20-9
(1R,3R,4S)-8-phenylmenthyl glyoxylate

Guidance literature:: With tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In benzene; at 20 ℃;
DOI:10.1016/j.tet.2006.06.118

Reference yield:

: 215321-43-0
Chloro-oxo-acetic acid (1R,2S,5R)-5-methyl-2-(1-methyl-1-phenyl-ethyl)-cyclohexyl ester

: 212073-12-6
(-)-(1R)-8-phenylmenthyl (1S,3-exo)-2-benzyl-2-azabicyclo[2.2.1]hept-5-ene-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: tributyltin hydride / tetrakis(triphenylphosphine)palladium⁽⁰⁾ / benzene / 20 °C

2: 80 percent / trifluoroacetic acid; BF₃*OEt₂; molecular sieves 3 Angstroem / CH₂Cl₂ / 6 h / -78 °C

With 3 A molecular sieve; boron trifluoride diethyl etherate; tri-n-butyl-tin hydride; trifluoroacetic acid; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; benzene;
DOI:10.1016/j.tet.2006.06.118