1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime

Base Information

Chemical Name:1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime
CAS No.:84736-67-4
Molecular Formula:C₂₅H₂₅Cl₂NO₂S
Molecular Weight:474.451
Hs Code.:

Synonyms:1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime

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Chemical Property of 1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime

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Technology Process of 1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime

There total 3 articles about 1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 100-39-0
benzyl bromide

: 84736-63-0
1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone oxime

: 84736-67-4
1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime

Guidance literature:: With sodium hydroxide; benzyltriethylammonium bromide; In dichloromethane; for 48h; Ambient temperature;
DOI:10.1055/s-1982-30001

Reference yield:

: 1519-39-7
(R)-methyl p-tolyl sulfoxide

: 84736-67-4
1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium diizopropylamide / 1.) THF, hexane, -70 -> -20 deg C, 2.) -78 deg C, 30 min

2: 49 percent / 10percent NaOH / benzyltriethylammonium bromide / CH₂Cl₂ / 48 h / Ambient temperature

With sodium hydroxide; lithium diisopropyl amide; benzyltriethylammonium bromide; In dichloromethane;
DOI:10.1055/s-1982-30001

Reference yield:

: 13456-86-5
3,5-Dichloro-2,4,6-trimethyl-benzonitrile N-oxide

: 84736-67-4
1-(3,5-Dichloro-2,4,6-trimethyl-phenyl)-2-((R)-toluene-4-sulfinyl)-ethanone O-benzyl-oxime

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) lithium diizopropylamide / 1.) THF, hexane, -70 -> -20 deg C, 2.) -78 deg C, 30 min

2: 49 percent / 10percent NaOH / benzyltriethylammonium bromide / CH₂Cl₂ / 48 h / Ambient temperature

With sodium hydroxide; lithium diisopropyl amide; benzyltriethylammonium bromide; In dichloromethane;
DOI:10.1055/s-1982-30001