phenylthallium(III) bis(trichloroacetate)

Base Information

Chemical Name:phenylthallium(III) bis(trichloroacetate)
CAS No.:73526-88-2
Molecular Formula:C₁₀H₅Cl₆O₄Tl
Molecular Weight:606.248
Hs Code.:

Synonyms:phenylthallium(III) bis(trichloroacetate)

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Chemical Property of phenylthallium(III) bis(trichloroacetate)

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Technology Process of phenylthallium(III) bis(trichloroacetate)

There total 2 articles about phenylthallium(III) bis(trichloroacetate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: thallium(III) oxide

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

: 76-03-9
trichloroacetic acid

: 73526-88-2
phenylthallium(III) bis(trichloroacetate)

Guidance literature:: In neat (no solvent); The mixt. of reagents was stirred at 70°C for 5 h, cooled to room temp.;; ppt. was filtered, washed with benzene, dried in vac. over silica gel; elem. anal.;;

Reference yield:

: thallium (III) oxide

: 76-03-9
trichloroacetic acid

: 73526-88-2
phenylthallium(III) bis(trichloroacetate)

Guidance literature:: With benzene; according to Uemura, S., et al., Bull. Soc. Jpn., 53, 553 (1980);

Reference yield: 76.2%

: 73526-88-2
phenylthallium(III) bis(trichloroacetate)

: 126583-54-8
(trichloroacetoxy)diphenylthallium

Guidance literature:: In acetone; byproducts: Tl(OCOCCl3)3; heating (1 h, water bath); evapn. (vac., room temp.), pptn. on addn. of water, filtration off, washing (water), drying (vac., 50°C); elem. anal.;