1-[dicarbonyl(η5-cyclopentadienyliron)]-2-phenyltetramethyldisilane

Base Information

Chemical Name:1-[dicarbonyl(η5-cyclopentadienyliron)]-2-phenyltetramethyldisilane
CAS No.:120547-10-6
Molecular Formula:C₁₇H₂₂FeO₂Si₂
Molecular Weight:370.378
Hs Code.:

Synonyms:1-[dicarbonyl(η5-cyclopentadienyliron)]-2-phenyltetramethyldisilane

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Chemical Property of 1-[dicarbonyl(η5-cyclopentadienyliron)]-2-phenyltetramethyldisilane

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Technology Process of 1-[dicarbonyl(η5-cyclopentadienyliron)]-2-phenyltetramethyldisilane

There total 1 articles about 1-[dicarbonyl(η5-cyclopentadienyliron)]-2-phenyltetramethyldisilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 38117-54-3
cyclopentadienyl iron(II) dicarbonyl dimer

: 4342-61-4
1,2-dichlorotetramethylsilane

: 108-90-7
chlorobenzene

: 120547-10-6
1-[dicarbonyl(η5-cyclopentadienyliron)]-2-phenyltetramethyldisilane

Guidance literature:: With (C₄H₉)4NBr; Mg; In tetrahydrofuran; byproducts: MgCl2; Electrolysis; N2; electrolysis of chlorobenzene and silane for 24 h at 25 mA with a magnesium anode, addn. of iron complex, electrolysis for 5 h (current density 1 mA cm**-2) in the presence of Bu4NBr (0.02 mol/l); removal of volatiles under reduced pressure, addn. of anhyd. pentane, filtration, washing with pentane, evapn., dissolving in toluene, chromy. (silica gel), removal of toluene;
DOI:10.1016/S0022-328X(02)02113-7