(1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate

Base Information

• Chemical Name: (1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate
• CAS No.: 226386-40-9
• Molecular Formula: C₁₆H₁₆N₄O₄
• Molecular Weight: 328.327
• Mol file: 226386-40-9.mol

Synonyms:(1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate

Chemical Property of (1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate

There total 3 articles about (1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

acetic anhydride (108-24-7) + orthoformic acid triethyl ester (122-51-0) + 6-amino-5-(benzylideneamino)-1,3-dimethyluracil → (1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate (226386-40-9)

Guidance literature:

1.) 100 deg C, 1 h, 2.) reflux, overnight;

DOI:10.1135/cccc19990313

Reference yield: 5.0%

diethoxymethyl acetate (14036-06-7) + 6-amino-5-(benzylideneamino)-1,3-dimethyluracil → 1,3-Dimethyl-6-phenylpyrazino<2,3-d>pyrimidine-2,4(1H,3H)-dione (25477-76-3) + (1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate (226386-40-9)

Guidance literature:

1.) r.t., 10 min, 2.) 100 deg C, 2 h;

DOI:10.1135/cccc19990313

Reference yield:

→ (1,3-Dimethyl-2,6(1H,3H)-dioxopurin-7-yl)(phenyl)methyl acetate (226386-40-9)

Guidance literature:

upstream raw materials:

diethoxymethyl acetate

acetic anhydride

orthoformic acid triethyl ester

Downstream raw materials:

theophylline