ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate

Base Information

Chemical Name:ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate
CAS No.:1018831-19-0
Molecular Formula:C₁₉H₁₉BrF₃NO₄S
Molecular Weight:494.329
Hs Code.:

Synonyms:ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate

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Chemical Property of ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate

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Technology Process of ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate

There total 1 articles about ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1018831-17-8
C₁₉H₂₀F₃NO₄S

: 1018831-19-0
ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate

Guidance literature:: With N-Bromosuccinimide; acetic acid; In dichloromethane; at -18 - -16 ℃; for 0.5h;
DOI:10.1016/j.bmc.2007.10.065

Reference yield: 96.0%

: 1018831-19-0
ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate

: 1679-18-1
4-Chlorophenylboronic acid

: 1053172-42-1
C₂₅H₂₃ClF₃NO₄S

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 70 - 80 ℃; for 24h;
DOI:10.1016/j.bmc.2007.10.065

Reference yield: 93.0%

: 1018831-19-0
ethyl 5-bromo-2-(tert-butoxycarbonylamino)-4-(3-(trifluoromethyl)phenyl)thiophene-3-carboxylate

: 149104-90-5
4-acetylphenylboronic acid

: 1053172-40-9
C₂₇H₂₆F₃NO₅S

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; N,N-dimethyl-formamide; at 70 - 80 ℃; for 24h;
DOI:10.1016/j.bmc.2007.10.065