5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol

Base Information

Chemical Name:5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol
CAS No.:1260432-94-7
Molecular Formula:C₁₈H₁₈BrN₃OS
Molecular Weight:404.33
Hs Code.:

Synonyms:5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol

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Technology Process of 5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol

There total 4 articles about 5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1260432-93-6
(3-bromophenyl)(4-methoxy-3,5-dimethylphenyl)methanimine

: 79-40-3
dithiooxamide

: 1260432-94-7
5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol

Guidance literature:: In ethanol; at 165 ℃; for 2h; Microwave irradiation;

Reference yield:

: 14804-38-7
5-bromo-2-methoxy-1,3-dimethylbenzene

: 1260432-94-7
5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol

Guidance literature:: Multi-step reaction with 3 steps

1.1: N,N-dimethyl-formamide / 136 °C

2.1: n-butyllithium / diethyl ether / 0.5 h / -78 °C

2.2: 0.5 h / -78 - 20 °C

3.1: ethanol / 2 h / 165 °C / Microwave irradiation

With n-butyllithium; In diethyl ether; ethanol; N,N-dimethyl-formamide;

Reference yield:

: 108-36-1
1,3-dibromobenzene

: 1260432-94-7
5-amino-2-(3-bromophenyl)-2-(4-methoxy-3,5-dimethylphenyl)-2H-imidazole-4-thiol

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / diethyl ether / 0.5 h / -78 °C

1.2: 0.5 h / -78 - 20 °C

2.1: ethanol / 2 h / 165 °C / Microwave irradiation

With n-butyllithium; In diethyl ether; ethanol;