N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine

Base Information

Chemical Name:N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine
CAS No.:1198077-72-3
Molecular Formula:C₃₁H₄₅NO₄Si
Molecular Weight:523.788
Hs Code.:

Synonyms:N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine

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Technology Process of N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine

There total 1 articles about N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 1198077-71-2
((7S,8S)-8-(benzyl(tert-butyldimethylsilyloxy)amino)-5,5-dimethyl-2,3,4,5,7,8-hexahydropyrano[4,3-b]pyran-7-yl)methanol

: 100-39-0
benzyl bromide

: 1198077-72-3
N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine

Guidance literature:: ((7S,8S)-8-(benzyl(tert-butyldimethylsilyloxy)amino)-5,5-dimethyl-2,3,4,5,7,8-hexahydropyrano[4,3-b]pyran-7-yl)methanol; With sodium hydride; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;

benzyl bromide; In tetrahydrofuran; mineral oil; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol902354f

Reference yield: 88.0%

: 1198077-72-3
N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine

: 1198077-73-4
(3S,4S)-3-[benzyl(tert-butyldimethylsiloxy)amino]-4-(benzyloxymethyl)-6,6-dimethyl-1,5-dioxecane-2,7-dione

Guidance literature:: With ruthenium trichloride; sodium periodate; water; In tetrachloromethane; acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/ol902354f

Reference yield: 88.0%

: 1198077-72-3
N-benzyl-N-((7S,8S)-7-(benzyloxymethyl)-5,5-dimethyl-3,4,5,6,7,8-hexahydropyrano[4,3-b]pyran-8-yl)-O-(tert-butyldimethylsilyl)hydroxylamine

: (3S,4S)-3-[benzyl(tert-butyldimethylsilyloxy)amino]-4(benzyloxymethyl)-6,6-dimethyl-1,5-dioxecane-2,7-dione

Guidance literature:: With ruthenium trichloride; sodium periodate; In tetrachloromethane; water; acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.3762/bjoc.6.75