C₁₅H₂₂O₃

Base Information

Chemical Name:C₁₅H₂₂O₃
CAS No.:1122481-07-5
Molecular Formula:C₁₅H₂₂O₃
Molecular Weight:250.338
Hs Code.:

C<sub>15</sub>H<sub>22</sub>O<sub>3</sub>

Synonyms:C₁₅H₂₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₅H₂₂O₃

Chemical Property:

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Technology Process of C₁₅H₂₂O₃

There total 1 articles about C₁₅H₂₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 547-63-7,133320-07-7,67505-84-4
Methyl isobutyrate

: 54314-84-0
1-[(3-bromopropoxy)methyl]-benzene

: 1122481-07-5
C₁₅H₂₂O₃

Guidance literature:: Methyl isobutyrate; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.333333h; Inert atmosphere;

1-[(3-bromopropoxy)methyl]-benzene; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at -78 ℃; for 12h; Inert atmosphere;
DOI:10.1021/ol802772s

Reference yield: 82.0%

: 1122481-07-5
C₁₅H₂₂O₃

: 1822-00-0
trimethylsilylmethyllithium

: 1122481-09-7
C₁₅H₂₂O₂

Guidance literature:: C₁₅H₂₂O₃; trimethylsilylmethyllithium; In pentane; at 0 ℃; for 4h; Inert atmosphere;

With methanol; In pentane; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol802772s

Reference yield:

: 1122481-07-5
C₁₅H₂₂O₃

: 1122481-17-7
C₄₆H₇₈O₇Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: pentane / 0 °C

1.2: 0 - 20 °C

2.1: triethylamine / dichloromethane / 0 - 20 °C

3.1: boron trifluoride diethyl etherate / dichloromethane / -78 °C

4.1: benzo[1,3,2]dioxaborole / tetrahydrofuran / -78 - 0 °C

4.2: 20 °C

With boron trifluoride diethyl etherate; triethylamine; benzo[1,3,2]dioxaborole; In tetrahydrofuran; dichloromethane; pentane;