syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II)

Base Information

• Chemical Name: syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II)
• CAS No.: 756499-10-2
• Molecular Formula: C₆₈H₄₆N₄P₂Zn
• Molecular Weight: 1046.48

Synonyms:syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II)

Chemical Property of syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II)

Chemical Property:

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Technology Process of syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II)

There total 1 articles about syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

syn-(5,15-bis[3'-(diphenylphosphinothioyl)biphenyl-2-yl]porphyrinato)zinc(II) * 2CH2Cl2 → syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II) (756499-10-2)

Guidance literature:

With chlorohydridobis(cyclopentadienyl)zirconium; In tetrahydrofuran; mixt. of Zn porphyrin complex and ZrH(C5H5)2Cl in THF stirred at 60°C for 3 h under N2; concd. in vacuo, flash chromy. on silica gel under N2;

DOI:10.1021/om0498201

Reference yield: 49.0%

dichloro bis(acetonitrile) palladium(II) (21264-30-2,90243-59-7,14592-56-4) + dichloromethane (75-09-2) + syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II) (756499-10-2) → ((C20H10N4(C6H4C6H4P(C6H5)2)2)Zn)PdCl2*2CH2Cl2

Guidance literature:

In benzene; mixt. of complexes in benzene stirred at room temp. for 8 h; evapd. in vacuo, residue recrystd. from CH2Cl2/hexane; elem. anal.;

DOI:10.1021/om0498201

Reference yield: 30.0%

bis(benzonitrile)dichloroplatinum(II) (14873-63-3,15617-19-3,51921-56-3) + chloroform (67-66-3,8013-54-5) + syn-(5,15-bis[3'-(diphenylphosphinyl)biphenyl-2-yl]porphyrinato)zinc(II) (756499-10-2) → ((C20H10N4(C6H4C6H4P(C6H5)2)2)Zn)PtCl2*2CHCl3

Guidance literature:

In dichloromethane; mixt. of complexes in CH2Cl2 stirred at room temp. for 5 h; evapd. in vacuo, residue recrystd. from CHCl3/hexane; elem. anal.;

DOI:10.1021/om0498201

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