N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

Base Information

Chemical Name:N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester
CAS No.:625117-31-9
Molecular Formula:C₁₈H₂₅NO₅S
Molecular Weight:367.466
Hs Code.:

Synonyms:N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

Suppliers and Price of N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

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Technology Process of N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

There total 5 articles about N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1,1-dioxo-N-(2,6-dimethylphenyl)-2H-thiopyran-4-amine

: 105-36-2
ethyl bromoacetate

: 625117-31-9
N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

Guidance literature:: 1,1-dioxo-N-(2,6-dimethylphenyl)-2H-thiopyran-4-amine; With potassium tert-butylate; In tetrahydrofuran; at 20 ℃; for 1h;

ethyl bromoacetate; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield: 89.0%

: 1,1-dioxo-N-(2,6-dimethylphenyl)-2H-thiopyran-4-amine

: 105-39-5
chloroacetic acid ethyl ester

: 625117-31-9
N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

Guidance literature:: 1,1-dioxo-N-(2,6-dimethylphenyl)-2H-thiopyran-4-amine; With potassium hydroxide; In tetrahydrofuran; at 20 ℃; for 1h;

chloroacetic acid ethyl ester; In tetrahydrofuran; at 20 ℃; for 3h;

Reference yield:

: 87-62-7
2,6-dimethylaniline

: 625117-31-9
N-(2,6-dimethylphenyl)-N-(1,1-dioxohexahydropyran-4-formyl)glycine ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetyl chloride / tetrahydrofuran / 3 h / 30 °C

2.1: potassium tert-butylate / tetrahydrofuran / 1 h / 20 °C

2.2: 3 h / 20 °C

With potassium tert-butylate; acetyl chloride; In tetrahydrofuran;