(4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole

Base Information

• Chemical Name: (4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole
• CAS No.: 93740-68-2
• Molecular Formula: C₂₈H₂₇NO₂
• Molecular Weight: 409.528

Synonyms:(4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole

Chemical Property of (4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole

Chemical Property:

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Technology Process of (4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole

There total 1 articles about (4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(4S,5S)-4-Methoxymethyl-2-naphthalen-2-yl-5-phenyl-4,5-dihydro-oxazole (93740-65-9) + phenyllithium (591-51-5) + methyl iodide (74-88-4) → (4S,5S)-4-Methoxymethyl-2-((1R,2S)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole (93781-29-4) + (4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole (93740-68-2)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given; 1.) -30 deg C 5 h 2.) -78 deg C_. ee = 80percent;

DOI:10.1016/0040-4039(84)80100-8

Reference yield:

Methyl fluorosulfonate (421-20-5) + (4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole (93740-68-2) → C29H30NO2(1+)*FO3S(1-)

Guidance literature:

In dichloromethane; at 25 ℃; for 15h;

DOI:10.1016/0040-4039(84)80100-8

Reference yield:

trimethoxonium tetrafluoroborate (420-37-1) + (4S,5S)-4-Methoxymethyl-2-((1S,2R)-2-methyl-1-phenyl-1,2-dihydro-naphthalen-2-yl)-5-phenyl-4,5-dihydro-oxazole (93740-68-2) → C29H30NO2(1+)*BF4(1-)

Guidance literature:

In dichloromethane; for 8h;

DOI:10.1016/0040-4039(84)80100-8

upstream raw materials:

(4S,5S)-4-Methoxymethyl-2-naphthalen-2-yl-5-phenyl-4,5-dihydro-oxazole

phenyllithium

methyl iodide

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