Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

Base Information

• Chemical Name: Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester
• CAS No.: 286949-86-8
• Molecular Formula: C₃₁H₄₆N₂O₂
• Molecular Weight: 478.718

Synonyms:Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

Chemical Property of Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

Chemical Property:

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Technology Process of Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

There total 1 articles about Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

vitamin D3 (67-97-0) + 1,1'-carbonyldiimidazole (530-62-1) → Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester (286949-86-8)

Guidance literature:

With triethylamine; In dichloromethane; for 2h; Heating;

DOI:10.1016/S0960-894X(00)00127-X

Reference yield:

N,N-dimethylethylenediamine (108-00-9) + Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester (286949-86-8) → (2-Dimethylamino-ethyl)-carbamic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

Guidance literature:

In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/S0960-894X(00)00127-X

Reference yield:

1,4-diaminobutane (110-60-1) + Imidazole-1-carboxylic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester (286949-86-8) → (4-Amino-butyl)-carbamic acid (S)-3-[2-[(1R,3aS,7aR)-1-((R)-1,5-dimethyl-hexyl)-7a-methyl-octahydro-inden-(4E)-ylidene]-eth-(Z)-ylidene]-4-methylene-cyclohexyl ester

Guidance literature:

In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/S0960-894X(00)00127-X

upstream raw materials:

vitamin D₃

1,1'-carbonyldiimidazole

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