C₅₈H₅₂O₇

Base Information

• Chemical Name: C₅₈H₅₂O₇
• CAS No.: 858127-48-7
• Molecular Formula: C₅₈H₅₂O₇
• Molecular Weight: 861.047
• Mol file: 858127-48-7.mol

Synonyms:C₅₈H₅₂O₇

Chemical Property of C₅₈H₅₂O₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₅₈H₅₂O₇

There total 5 articles about C₅₈H₅₂O₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

5-[(4-vinylbenzyloxy)methyl]benzene-1,3-diol (858127-47-6) + 3,5-bis(benzyloxy)benzyl bromide (24131-32-6) → C58H52O7 (858127-48-7)

Guidance literature:

With 18-crown-6 ether; potassium carbonate; potassium iodide; In acetone; for 48h; Heating;

DOI:10.1021/ma047449n

Reference yield:

2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran (858127-53-4) → C58H52O7 (858127-48-7)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrochloric acid / methanol; CH₂Cl₂; H₂O / 3 h / 20 °C

2: 69 percent / potassium carbonate; potassium iodide; 18-crown-6 / acetone / 48 h / Heating

With hydrogenchloride; 18-crown-6 ether; potassium carbonate; potassium iodide; In methanol; dichloromethane; water; acetone;

DOI:10.1021/ma047449n

Reference yield:

3,5-bis(tetrahydropyran-2-yloxy)benzoic acid methyl ester (33617-41-3) → C58H52O7 (858127-48-7)

Guidance literature:

Multi-step reaction with 4 steps

1: LiAlH₄ / tetrahydrofuran / 4 h / Heating

2: 78 percent / sodium hydride; 18-crown-6 / tetrahydrofuran / 24 h / Heating

3: hydrochloric acid / methanol; CH₂Cl₂; H₂O / 3 h / 20 °C

4: 69 percent / potassium carbonate; potassium iodide; 18-crown-6 / acetone / 48 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; 18-crown-6 ether; sodium hydride; potassium carbonate; potassium iodide; In tetrahydrofuran; methanol; dichloromethane; water; acetone; 2: Williamson reaction;

DOI:10.1021/ma047449n

upstream raw materials:

5-[(4-vinylbenzyloxy)methyl]benzene-1,3-diol

3,5-bis(benzyloxy)benzyl bromide

2-{3-[(4-vinylbenzyloxy)methyl]-5-(tetrahydro-2H-pyran-2-yloxy)phenoxy}tetrahydro-2H-pyran

(3,5-bis(tetrahydro-2H-pyran-2-yloxy)phenyl)methanol