{4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone

Base Information

Chemical Name:{4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone
CAS No.:1160829-36-6
Molecular Formula:C₂₄H₂₉N₅O
Molecular Weight:403.527
Hs Code.:

Synonyms:{4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone

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Chemical Property of {4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone

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Technology Process of {4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone

There total 1 articles about {4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 2-(3-piperazin-1-yl-phenyl)-1H-benzoimidazole dihydrochloride

: 71985-80-3,71235-92-2
1-methylpiperidine-4-carboxylic acid hydrochloride

: 1160829-36-6
{4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone

Guidance literature:: 1-methylpiperidine-4-carboxylic acid hydrochloride; With N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; In acetonitrile; at 20 ℃; for 5h;

2-(3-piperazin-1-yl-phenyl)-1H-benzoimidazole dihydrochloride; In acetonitrile; at 65 ℃;

Reference yield: 69.0%

: 64-18-6
formic acid

: 1160829-36-6
{4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone

: 2-{3-[4-(1-methyl-piperidin-4-ylmethyl)-piperazin-1-yl]-phenyl}-1H-benzoimidazole formate

Guidance literature:: {4-[3-(1H-benzoimidazol-2-yl)-phenyl]-piperazin-1-yl}-(1-methyl-piperidin-4-yl)-methanone; With dimethylsulfide borane complex; In tetrahydrofuran; at 60 ℃;

With hydrogenchloride; water; at 100 ℃; for 5h;

formic acid; With sodium hydroxide; water; more than 3 stages;