2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole

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Chemical Name:2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole
CAS No.:896138-55-9
Molecular Formula:C₁₈H₁₈N₂O
Molecular Weight:278.354
Hs Code.:

Synonyms:2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole

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Chemical Property of 2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole

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Technology Process of 2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole

There total 4 articles about 2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 60658-98-2
3-methoxy-5-phenyl-1H-pyrrole-2-carbaldehyde

: 896138-55-9
2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole

Guidance literature:: With hydrogenchloride; In methanol; at 25 ℃; for 5h; Inert atmosphere;
DOI:10.1021/jm200543y

Reference yield:

: 803712-71-2
N-((5-bromo-3-methoxy-2H-pyrrol-2-ylidene)-methyl)-N-ethylethanamine

: 896138-55-9
2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium diacetate; triphenylphosphine / 1,4-dioxane; water; toluene / 70 °C / Inert atmosphere

1.2: 3 h / 100 °C / Inert atmosphere

2.1: hydrogenchloride / methanol / 5 h / 25 °C / Inert atmosphere

With hydrogenchloride; palladium diacetate; triphenylphosphine; In 1,4-dioxane; methanol; water; toluene;
DOI:10.1021/jm200543y

Reference yield:

: 23999-91-9
1H-pyrrole-2,4-dicarboxaldehyde

: 896138-55-9
2-((3-methoxy-5-phenyl-2H-pyrrol-2-ylidene)methyl)-3,5-dimethyl-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / isopropyl alcohol / 10 h / Reflux

2: hydrogenchloride / methanol / 5 h / 25 °C / Inert atmosphere

With hydrogenchloride; sodium tetrahydroborate; In methanol; isopropyl alcohol;
DOI:10.1021/jm200543y