2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline

Base Information

Chemical Name:2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline
CAS No.:1150647-60-1
Molecular Formula:C₂₅H₃₃Br₂N
Molecular Weight:507.352
Hs Code.:

Synonyms:2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline

Chemical Property:

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Technology Process of 2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline

There total 6 articles about 2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1150647-48-5
2-benzyl-1,1,3,3-tetraethyl-5,6-bis(hydroxymethyl)isoindoline

: 1150647-60-1
2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline

Guidance literature:: With phosphorus tribromide; In dichloromethane; for 1.5h; Inert atmosphere; Cooling with ice;
DOI:10.1002/ejoc.200801255

Reference yield:

: 1150647-47-4
2-benzoyl-1,1,3,3-tetraethylisoindoline-5,6-dicarboxylic acid

: 1150647-60-1
2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / diethyl ether / 72 h / Reflux

2: phosphorus tribromide / dichloromethane / 1.5 h / Inert atmosphere; Cooling with ice

With lithium aluminium tetrahydride; phosphorus tribromide; In diethyl ether; dichloromethane;

Reference yield:

: 5999-20-2
4,5-dimethylphthalic anhydride

: 1150647-60-1
2-benzyl-5,6-bis(bromomethyl)-1,1,3,3-tetraethylisoindoline

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid / 1.5 h / 120 °C

2: toluene; diethyl ether / 3 h / Reflux

3: sodium hydroxide; pyridine; potassium permanganate / water / 96 h / Reflux

4: lithium aluminium tetrahydride / diethyl ether / 72 h / Reflux

5: phosphorus tribromide / dichloromethane / 1.5 h / Inert atmosphere; Cooling with ice

With pyridine; potassium permanganate; lithium aluminium tetrahydride; phosphorus tribromide; acetic acid; sodium hydroxide; In diethyl ether; dichloromethane; water; toluene;