2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline

Base Information

Chemical Name:2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline
CAS No.:1150647-62-3
Molecular Formula:C₂₅H₃₇NO₆P₂
Molecular Weight:509.519
Hs Code.:

Synonyms:2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline

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Chemical Property of 2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline

Chemical Property:

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Technology Process of 2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline

There total 8 articles about 2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1150647-61-2
2-benzyl-5,6-bis(diethoxyphosphorylmethyl)-1,1,3,3-tetraethylisoindoline

: 1150647-62-3
2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline

Guidance literature:: With hydrogenchloride; In water; for 16h; Reflux;
DOI:10.1002/ejoc.200801255

Reference yield:

: 100-46-9
benzylamine

: 1150647-62-3
2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid / 1.5 h / 120 °C

2: toluene; diethyl ether / 3 h / Reflux

3: sodium hydroxide; pyridine; potassium permanganate / water / 96 h / Reflux

4: lithium aluminium tetrahydride / diethyl ether / 72 h / Reflux

5: phosphorus tribromide / dichloromethane / 1.5 h / Inert atmosphere; Cooling with ice

6: 16 h / 80 °C

7: hydrogenchloride; water / 16 h / Reflux

With pyridine; hydrogenchloride; potassium permanganate; lithium aluminium tetrahydride; water; phosphorus tribromide; acetic acid; sodium hydroxide; In diethyl ether; dichloromethane; water; toluene;

Reference yield:

: 5999-20-2
4,5-dimethylphthalic anhydride

: 1150647-62-3
2-benzyl-1,1,3,3-tetraethyl-5,6-bis(phosphonomethyl)isoindoline

Guidance literature:: Multi-step reaction with 7 steps

1: acetic acid / 1.5 h / 120 °C

2: toluene; diethyl ether / 3 h / Reflux

3: sodium hydroxide; pyridine; potassium permanganate / water / 96 h / Reflux

4: lithium aluminium tetrahydride / diethyl ether / 72 h / Reflux

5: phosphorus tribromide / dichloromethane / 1.5 h / Inert atmosphere; Cooling with ice

6: 16 h / 80 °C

7: hydrogenchloride; water / 16 h / Reflux

With pyridine; hydrogenchloride; potassium permanganate; lithium aluminium tetrahydride; water; phosphorus tribromide; acetic acid; sodium hydroxide; In diethyl ether; dichloromethane; water; toluene;