ethyl 4-methoxyphenyl chlorothiophosphate

Base Information

• Chemical Name: ethyl 4-methoxyphenyl chlorothiophosphate
• CAS No.: 83485-45-4
• Molecular Formula: C₉H₁₂ClO₃PS
• Molecular Weight: 266.685
• Mol file: 83485-45-4.mol

Synonyms:ethyl 4-methoxyphenyl chlorothiophosphate

Chemical Property of ethyl 4-methoxyphenyl chlorothiophosphate

Chemical Property:

Purity/Quality:

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Technology Process of ethyl 4-methoxyphenyl chlorothiophosphate

There total 1 articles about ethyl 4-methoxyphenyl chlorothiophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

O-ethyl dichlorothiophosphate (1498-64-2) + 4-methoxy-phenol (150-76-5) → ethyl 4-methoxyphenyl chlorothiophosphate (83485-45-4)

Guidance literature:

With triethylamine; In dichloromethane; for 2h; cooling;

DOI:10.1039/b713167d

Reference yield: 78.9%

ethyl 4-methoxyphenyl chlorothiophosphate (83485-45-4) + (S)-10-hydroxycamptothecin (19685-09-7,64439-81-2) → C29H27N2O8PS (1381809-43-3)

Guidance literature:

(S)-10-hydroxycamptothecin; With sodium hydroxide; In acetonitrile; at 24.84 ℃;

ethyl 4-methoxyphenyl chlorothiophosphate; In acetonitrile; at 60 ℃; Inert atmosphere;

DOI:10.1080/10426507.2011.631643

Reference yield:

ethyl 4-methoxyphenyl chlorothiophosphate (83485-45-4) + p-anisidine-ND2 (45714-57-6) → C16H19(2)HNO4PS

Guidance literature:

In acetonitrile; at 55 ℃; Kinetics;

DOI:10.1039/b713167d

upstream raw materials:

O-ethyl dichlorothiophosphate

4-methoxy-phenol

Downstream raw materials:

C₂₉H₂₇N₂O₈PS