1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane

Base Information

Chemical Name:1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane
CAS No.:1621596-23-3
Molecular Formula:C₁₆H₂₂B₁₀N₂O₂S
Molecular Weight:414.539
Hs Code.:

Synonyms:1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane

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Chemical Property of 1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane

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Technology Process of 1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane

There total 1 articles about 1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1621596-16-4
1-(4-cyanophenyl)-12-phenyl-1,12-dicarba-closo-dodecaborane

: 124-63-0
methanesulfonyl chloride

: 1621596-23-3
1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane

Guidance literature:: 1-(4-cyanophenyl)-12-phenyl-1,12-dicarba-closo-dodecaborane; With sulfuric acid; nitric acid; In dichloromethane; at 0 ℃; for 1h;

With palladium on activated charcoal; hydrogen; In ethyl acetate; for 4h;

methanesulfonyl chloride; In pyridine; dichloromethane; at 0 - 20 ℃; for 2.5h;
DOI:10.1016/j.ejmech.2014.07.034

Reference yield: 50.0%

: 1621596-23-3
1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane

: 74-88-4
methyl iodide

: 1621596-25-5
1-(4-cyanophenyl)-12-(4-N-methylmethylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane

Guidance literature:: 1-(4-cyanophenyl)-12-(4-methylsulfonamidophenyl)-1,12-dicarba-closo-dodecaborane; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.25h;

methyl iodide; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2.5h;
DOI:10.1016/j.ejmech.2014.07.034