ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate

Base Information

Chemical Name:ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate
CAS No.:911381-06-1
Molecular Formula:C₂₄H₂₄F₆N₂O₄
Molecular Weight:518.456
Hs Code.:

Synonyms:ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate

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Chemical Property of ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate

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Technology Process of ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate

There total 5 articles about ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 911381-05-0
2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethyl methanesulfonate

: 197299-16-4
ethyl 2-ethoxy-3-(4-hydroxy-phenyl)-propionate

: 911381-06-1
ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate

Guidance literature:: With potassium carbonate; In toluene; for 30h; Heating / reflux;

Reference yield:

: 367-86-2
1-fluoro-2-nitro-4-trifluoromethyl-benzene

: 911381-06-1
ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate

Guidance literature:: Multi-step reaction with 5 steps

1: tetrahydrofuran / 24 h / 0 - 20 °C

2: hydrogen / tetrahydrofuran / 3620.13 Torr

3: dmap; triethylamine / dichloromethane / 0 - 20 °C

4: triethylamine / dichloromethane / 0 - 20 °C

5: potassium carbonate / toluene / 30 h / Heating / reflux

With dmap; hydrogen; potassium carbonate; triethylamine; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 911381-04-9
2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethanol

: 911381-06-1
ethyl 3-(4-{2-[2,5-bis(trifluoromethyl)-1H-benzimidazol-1-yl]ethoxy}phenyl)-2-ethoxypropanoate

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 0 - 20 °C

2: potassium carbonate / toluene / 30 h / Heating / reflux

With potassium carbonate; triethylamine; In dichloromethane; toluene;