2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Base Information

Chemical Name:2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone
CAS No.:65699-27-6
Molecular Formula:C₂₁H₁₈Cl₃N₅O₃
Molecular Weight:494.765
Hs Code.:

Synonyms:2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

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Chemical Property of 2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

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Technology Process of 2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

There total 8 articles about 2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 65699-26-5
2',5-dichloro-2-(3-dimethylcarbamoyl-5-aminomethyl-1H-1,2,4-triazol-1-yl)benzophenone hydrobromide

: 79-04-9
chloroacetyl chloride

: 65699-27-6
2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: In N,N-dimethyl-formamide; benzene; for 3h;
DOI:10.1002/jhet.5570190621

Reference yield:

: 50330-59-1
8-chloro-6-(2-chloro-phenyl)-4H-benzo[f][1,2,4]triazolo[1,5-a][1,4]diazepine-2-carboxylic acid dimethylamide

: 65699-27-6
2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: Multi-step reaction with 2 steps

1: aq. HBr / Heating

2: 90 percent / benzene; dimethylformamide / 3 h

With hydrogen bromide; In N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570190621

Reference yield:

: 65698-99-9
N,N-dimethyl 2-amino-2-(2-(2-chlorobenzoyl)-5-chlorophenylazo)acetamide

: 65699-27-6
2',5-dichloro-2-(3-dimethylcarbamoyl-5-chloroacetylaminomethyl-1H-1,2,4-triazol-1-yl)benzophenone

Guidance literature:: Multi-step reaction with 3 steps

1: 47 percent / K₂CO₃ / tetrahydrofuran; dimethylformamide / Ambient temperature; overnight

2: 30percent HBr/acetic acid / 2 h / Ambient temperature

3: 90 percent / benzene; dimethylformamide / 3 h

With hydrogen bromide; potassium carbonate; acetic acid; In tetrahydrofuran; N,N-dimethyl-formamide; benzene;
DOI:10.1002/jhet.5570190621