3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid

Base Information

Chemical Name:3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid
CAS No.:1426409-08-6
Molecular Formula:C₁₅H₁₇NO₅
Molecular Weight:291.304
Hs Code.:

Synonyms:3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid

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Chemical Property of 3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid

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Technology Process of 3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid

There total 5 articles about 3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 513-35-9
2-methyl-but-2-ene

: 1426409-07-5
3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carbaldehyde

: 1426409-08-6
3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate dihydrate; In tetrahydrofuran; water; tert-butyl alcohol; at 0 - 20 ℃; for 24h; Inert atmosphere;

Reference yield:

: 1426409-04-2
N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

: 1426409-08-6
3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: rhodium(II) acetate dimer; α,α,α-trifluorotoluene / 24 h / 50 °C / Inert atmosphere

2: tetranormalbutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

3: triethylamine; sulfur trioxide pyridine complex / chloroform; dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

4: sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 24 h / 0 - 20 °C / Inert atmosphere

With tetranormalbutyl ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate dihydrate; α,α,α-trifluorotoluene; rhodium(II) acetate dimer; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide; tert-butyl alcohol;

Reference yield:

: 1426409-05-3
5-(tert-butyldimethylsilanyloxymethyl)-3-(2,4-dimethoxybenzyl)-3-azabicyclo[3.1.0]hexan-2-one

: 1426409-08-6
3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: tetranormalbutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

2: triethylamine; sulfur trioxide pyridine complex / chloroform; dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

3: sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 24 h / 0 - 20 °C / Inert atmosphere

With tetranormalbutyl ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate dihydrate; sulfur trioxide pyridine complex; triethylamine; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide; tert-butyl alcohol;