[2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

Base Information

Chemical Name:[2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine
CAS No.:1426409-03-1
Molecular Formula:C₁₉H₃₃NO₃Si
Molecular Weight:351.561
Hs Code.:

Synonyms:[2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

Chemical Property:

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Technology Process of [2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

There total 1 articles about [2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1426409-03-1
[2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine; methanesulfonyl chloride / chloroform / 2 h / 0 °C

2.2: 15 h / 20 °C

With sodium hydride; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; chloroform; mineral oil;

Reference yield:

: 1426409-03-1
[2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

: 147666-20-4
succinimidyl diazoacetate

: 1426409-04-2
N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 16h;

Reference yield:

: 1426409-03-1
[2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

: 1426409-09-7
3-(2,4-dimethoxybenzyl)-4-oxo-3-azabicyclo[3.1.0]hexane-1-carboxylic acid[1-phenyl-5-(3-propylphenyl)-1H-pyrazol-3-yl]amide

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / chloroform / 16 h / 20 °C

2.1: rhodium(II) acetate dimer; α,α,α-trifluorotoluene / 24 h / 50 °C / Inert atmosphere

3.1: tetranormalbutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

4.1: triethylamine; sulfur trioxide pyridine complex / chloroform; dimethyl sulfoxide / 2 h / 20 °C / Inert atmosphere

5.1: sodium dihydrogenphosphate dihydrate; sodium chlorite / tetrahydrofuran; water; tert-butyl alcohol / 24 h / 0 - 20 °C / Inert atmosphere

6.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / N,N-dimethyl-formamide / 14 h / 20 °C

6.2: 72 h / 20 °C

With tetranormalbutyl ammonium fluoride; sodium chlorite; sodium dihydrogenphosphate dihydrate; α,α,α-trifluorotoluene; rhodium(II) acetate dimer; sulfur trioxide pyridine complex; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In tetrahydrofuran; chloroform; water; dimethyl sulfoxide; N,N-dimethyl-formamide; tert-butyl alcohol;