N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

Base Information

Chemical Name:N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide
CAS No.:1426409-04-2
Molecular Formula:C₂₁H₃₃N₃O₄Si
Molecular Weight:419.596
Hs Code.:

Synonyms:N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

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Technology Process of N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

There total 3 articles about N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1426409-03-1
[2-(tert-butyldimethylsilanyloxymethyl)allyl]-(2,4-dimethoxybenzyl)amine

: 147666-20-4
succinimidyl diazoacetate

: 1426409-04-2
N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

Guidance literature:: With triethylamine; In chloroform; at 20 ℃; for 16h;

Reference yield:

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1426409-04-2
N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine; methanesulfonyl chloride / chloroform / 2 h / 0 °C

2.2: 15 h / 20 °C

3.1: triethylamine / chloroform / 16 h / 20 °C

With sodium hydride; methanesulfonyl chloride; triethylamine; In tetrahydrofuran; chloroform; mineral oil;

Reference yield:

: 116700-73-3
2-(tert-butyl-dimethyl-silanyloxymethyl)-prop-2-en-1-ol

: 1426409-04-2
N-[2-(tert-butyldimethylsilanyloxymethyl)allyl]-2-diazo-N-(2,4-dimethoxybenzyl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; methanesulfonyl chloride / chloroform / 2 h / 0 °C

1.2: 15 h / 20 °C

2.1: triethylamine / chloroform / 16 h / 20 °C

With methanesulfonyl chloride; triethylamine; In chloroform;