[(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6

Base Information

Chemical Name:[(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6
CAS No.:717901-49-0
Molecular Formula:C₄₇H₄₆FeNP₂RuS*F₆P
Molecular Weight:1020.78
Hs Code.:

Synonyms:[(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6

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Chemical Property of [(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6

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Technology Process of [(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6

There total 1 articles about [(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 201543-21-7
[(η(6)-hexamethylbenzene)RuCl(1,1'-bis(diphenylphosphino)ferrocene-P,P')]PF6

: 540-72-7
sodium thiocyanide

: 717901-49-0
[(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6

Guidance literature:: In methanol; (N2); refluxing a mixt. of ruthenium complex with NaNCS in MeOH for 23 h; filtration, washing with MeOH, ether, drying in vac., evapn. of filtrate, recrystn. (CH2Cl2/hexane 1:4); elem. anal.;
DOI:10.1016/j.jorganchem.2004.03.022

Reference yield: 70.0%

: 717901-49-0
[(η6-hexamethylbenzene)Ru(1,1'-bis(diphenylphosphino)ferrocene)(NCS)]PF6

: 540-72-7
sodium thiocyanide

: 12150-46-8
1,1'-bis-(diphenylphosphino)ferrocene

: [(η6-hexamethylbenzene)Ru(NCS)2]2(μ-1,1'-bis(diphenylphosphino)ferrocene)

Guidance literature:: In acetonitrile; (N2); stirring a mixt. of ruthenium complex and NaNCS in acetonitrile for 2 d; filtration, concn., addn. of ether, cooling to 0°C for 3 h; elem.anal.;
DOI:10.1016/j.jorganchem.2004.03.022