1-benzyloxymethyl-cyclopentanecarbaldehyde

Base Information

Chemical Name:1-benzyloxymethyl-cyclopentanecarbaldehyde
CAS No.:941687-71-4
Molecular Formula:C₁₄H₁₈O₂
Molecular Weight:218.296
Hs Code.:

Synonyms:1-benzyloxymethyl-cyclopentanecarbaldehyde

Suppliers and Price of 1-benzyloxymethyl-cyclopentanecarbaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1-benzyloxymethyl-cyclopentanecarbaldehyde

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-benzyloxymethyl-cyclopentanecarbaldehyde

There total 3 articles about 1-benzyloxymethyl-cyclopentanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: (1-benzyloxymethyl-cyclopentyl)-methanol

: 941687-71-4
1-benzyloxymethyl-cyclopentanecarbaldehyde

Guidance literature:: (1-benzyloxymethyl-cyclopentyl)-methanol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 2h;

With triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1016/j.tet.2015.11.046

Reference yield:

: 5763-53-1
1,1-bis-(hydroxymethyl)cyclopentane

: 941687-71-4
1-benzyloxymethyl-cyclopentanecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 °C

2.2: -78 - 20 °C

With oxalyl dichloride; sodium hydride; dimethyl sulfoxide; In dichloromethane; N,N-dimethyl-formamide; mineral oil; 2.1: |Swern Oxidation / 2.2: |Swern Oxidation;
DOI:10.1016/j.tet.2015.11.046

Reference yield:

: 100-39-0
benzyl bromide

: 941687-71-4
1-benzyloxymethyl-cyclopentanecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0.75 h / 0 °C / Inert atmosphere

1.2: 0 - 20 °C / Inert atmosphere

2.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 2 h / -78 °C

2.2: -78 - 20 °C

With oxalyl dichloride; sodium hydride; dimethyl sulfoxide; In dichloromethane; N,N-dimethyl-formamide; mineral oil; 2.1: |Swern Oxidation / 2.2: |Swern Oxidation;
DOI:10.1016/j.tet.2015.11.046