Technology Process of C20H20FNO3
There total 5 articles about C20H20FNO3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
3-fluorobromobenzene;
With
magnesium;
In
diethyl ether;
for 2h;
Reflux;
C14H15NO3;
In
diethyl ether;
at 0 - 20 ℃;
for 2h;
DOI:10.1021/jm301588r
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium carbonate / methanol / 0.5 h / 120 °C / Microwave irradiation; Inert atmosphere
2.1: magnesium / diethyl ether / 2 h / Reflux
2.2: 2 h / 0 - 20 °C
With
potassium carbonate; magnesium;
In
methanol; diethyl ether;
DOI:10.1021/jm301588r
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Reflux
2.1: pyridinium chlorochromate / dichloromethane / 3.5 h / 0 - 20 °C
3.1: palladium diacetate; ruphos; sodium carbonate / ethanol / 2 h / Inert atmosphere; Reflux
4.1: potassium carbonate / methanol / 0.5 h / 120 °C / Microwave irradiation; Inert atmosphere
5.1: magnesium / diethyl ether / 2 h / Reflux
5.2: 2 h / 0 - 20 °C
With
lithium aluminium tetrahydride; palladium diacetate; sodium carbonate; potassium carbonate; magnesium; pyridinium chlorochromate; ruphos;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane;
DOI:10.1021/jm301588r
