3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid

Base Information

Chemical Name:3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid
CAS No.:1268476-87-4
Molecular Formula:C₂₁H₂₂N₂O₄
Molecular Weight:366.417
Hs Code.:

Synonyms:3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid

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Chemical Property of 3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid

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Technology Process of 3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid

There total 9 articles about 3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1268476-85-2
ethyl 3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylate

: 1268476-87-4
3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid

Guidance literature:: With water; sodium hydroxide; In ethanol; at 70 ℃; for 3h;

Reference yield:

: 1268476-81-8
ethyl 3-ethenyl-6-ethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo-[3,2-c]pyridine-2-carboxylate

: 1268476-87-4
3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 10 - 35 °C

2: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / acetonitrile / 1 h / 10 - 35 °C

3: sodium hydroxide; water / ethanol / 3 h / 70 °C

With tetrapropylammonium perruthennate; water; hydrogen; 4-methylmorpholine N-oxide; sodium hydroxide; palladium 10% on activated carbon; In methanol; ethanol; acetonitrile;

Reference yield:

: 30414-53-0
methyl propanoyl acetate

: 1268476-87-4
3,6-diethyl-1-methyl-4-oxo-5-(2-oxo-2-phenylethyl)-4,5-dihydro-1H-pyrrolo[3,2-c]-pyridine-2-carboxylic acid

Guidance literature:: Multi-step reaction with 10 steps

1: ammonium acetate / methanol / 72 h / 10 - 35 °C

2: sodium ethanolate / ethanol / 15 h / 150 °C

3: trichlorophosphate / 0.5 h / 80 °C

4: potassium carbonate / N,N-dimethyl-formamide / 15 h / 10 - 35 °C

5: triethylamine / ethanol / 25 h / 80 - 100 °C

6: pyridine / 3 h / 60 °C / Inert atmosphere

7: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water / 3 h / 100 °C / Inert atmosphere

8: hydrogen / palladium 10% on activated carbon / methanol / 2 h / 10 - 35 °C

9: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / acetonitrile / 1 h / 10 - 35 °C

10: sodium hydroxide; water / ethanol / 3 h / 70 °C

With pyridine; tetrapropylammonium perruthennate; ammonium acetate; water; hydrogen; sodium ethanolate; potassium carbonate; 4-methylmorpholine N-oxide; triethylamine; sodium hydroxide; trichlorophosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; In methanol; ethanol; water; N,N-dimethyl-formamide; acetonitrile;