5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene

Base Information

Chemical Name:5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene
CAS No.:98115-50-5
Molecular Formula:C₁₇H₂₀O₂
Molecular Weight:256.345
Hs Code.:

Synonyms:5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene

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Chemical Property of 5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene

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Technology Process of 5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene

There total 4 articles about 5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 98115-49-2
1-(4,4-ethylenedioxy-2-methylcyclohex-1-enylmethyl)-5-methoxy-1,2-dihydrocyclobutabenzene

: 98115-50-5
5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene

Guidance literature:: With hydrogenchloride; In methanol; for 5h; Ambient temperature;

Reference yield:

: 1199-31-1
1-cyano-5-methoxybenzocyclobutane

: 98115-50-5
5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 81 percent / LDA / tetrahydrofuran; hexamethylphosphoric acid triamide / 1 h / -78 °C

2: 73 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating

3: 80 percent / liq. NH₃, sodium / ethanol; tetrahydrofuran / 3 h / -78 °C

4: 78 percent / 10percent HCl / methanol / 5 h / Ambient temperature

With hydrogenchloride; ammonia; sodium; lithium diisopropyl amide; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; ethanol; benzene;

Reference yield:

: 98115-47-0
1-cyano-5-methoxy-1-(2-methyl-4-oxocyclohex-1-enylmethyl)-1,2-dihydrocyclobutabenzene

: 98115-50-5
5-methoxy-1-(2-methyl-4-oxocyclohex-2-enylmethyl)-1,2-dihydrocyclobutabenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating

2: 80 percent / liq. NH₃, sodium / ethanol; tetrahydrofuran / 3 h / -78 °C

3: 78 percent / 10percent HCl / methanol / 5 h / Ambient temperature

With hydrogenchloride; ammonia; sodium; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; benzene;