[Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]

Base Information

Chemical Name:[Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]
CAS No.:207297-58-3
Molecular Formula:C₃₁H₃₅O₉Rh
Molecular Weight:654.519
Hs Code.:

Synonyms:[Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]

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Chemical Property of [Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]

Chemical Property:

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Technology Process of [Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]

There total 3 articles about [Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: di(rhodium)tetracarbonyl dichloride

: 163930-26-5
2,4-Dioxo-3-pentyl 4-{[4-(n-decyloxy)benzoyl]oxy}benzoate

: 207297-58-3
[Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]

Guidance literature:: With barium carbonate; In acetone; N2-atmosphere; stirring Rh-complex with 2 equiv. of ligand and excess BaCO3 (room temp., 30 min); filtration, distn., chromy. (SiO2, CHCl3), recrystn. (EtOH); elem. anal.;
DOI:10.1016/S0022-328X(97)00653-0

Reference yield: 79.0%

: di(rhodium)tetracarbonyl dichloride

: 3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedione

: 207297-58-3
[Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]

Guidance literature:: With sodium acetate; In methanol; Ar-atmosphere; treatment of diketone with 1 equiv. AcONa, addn. of stoich. amt. of Rh-complex, stirring at room temp. for 1 h; pptn. on evapn.; elem. anal.;
DOI:10.1021/ic9814017

Reference yield:

: 12092-47-6
di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium

: 3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedione

: 201230-82-2
carbon monoxide

: 207297-58-3
[Rh(3-[(4'-((4''-n-decyloxybenzoyl)oxy)benzoyl)oxy]-2,4-pentanedionate)(CO)2]

Guidance literature:: With KOH; In methanol; diethyl ether; Ar-atmosphere; treatment of diketone (in MeOH) with KOH, addn. of Rh-complex (in Et2O), standing for 30 min; concn., pptn. on MeOH addn.;
DOI:10.1021/ic9814017