benzyl 2,4-dimethoxyphenylcarbamate

Base Information

• Chemical Name: benzyl 2,4-dimethoxyphenylcarbamate
• CAS No.: 1137558-12-3
• Molecular Formula: C₁₆H₁₇NO₄
• Molecular Weight: 287.315
• Mol file: 1137558-12-3.mol

Synonyms:benzyl 2,4-dimethoxyphenylcarbamate

Chemical Property of benzyl 2,4-dimethoxyphenylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzyl 2,4-dimethoxyphenylcarbamate

There total 1 articles about benzyl 2,4-dimethoxyphenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dimethoxyphenyl isocyanate (84370-87-6) + benzyl alcohol (100-51-6,185532-71-2) → benzyl 2,4-dimethoxyphenylcarbamate (1137558-12-3)

Guidance literature:

In benzene; Reflux;

DOI:10.1021/jm801335z

Reference yield: 94.0%

benzyl 2,4-dimethoxyphenylcarbamate (1137558-12-3) → 2,4-Dimethoxyaniline (2735-04-8,161687-55-4)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In ethyl acetate; for 6h; under 1551.49 Torr;

DOI:10.1021/jm801335z

Reference yield: 90.0%

benzyl 2,4-dimethoxyphenylcarbamate (1137558-12-3) + methyl iodide (74-88-4) → benzyl 2,4-dimethoxyphenyl(methyl)carbamate (1137558-19-0)

Guidance literature:

benzyl 2,4-dimethoxyphenylcarbamate; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1021/jm801335z

upstream raw materials:

2,4-dimethoxyphenyl isocyanate

benzyl alcohol

Downstream raw materials:

2,4-Dimethoxyaniline

benzyl 2,4-dimethoxyphenyl(methyl)carbamate