C₂₆H₃₆N₂

Base Information

• Chemical Name: C₂₆H₃₆N₂
• CAS No.: 144582-02-5
• Molecular Formula: C₂₆H₃₆N₂
• Molecular Weight: 376.585
• Mol file: 144582-02-5.mol

Synonyms:C₂₆H₃₆N₂

Chemical Property of C₂₆H₃₆N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₆H₃₆N₂

There total 13 articles about C₂₆H₃₆N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,4-bis-(3-bromopropyl)-benzene (19417-59-5) → C26H36N2 (144582-02-5)

Guidance literature:

Multi-step reaction with 8 steps

1: ethanol

2: aq. KOH

3: SOCl₂ / 0.5 h / Heating

4: 57 percent / SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

5: 80 percent / B₂H₆ / tetrahydrofuran

6: 86 percent / PhCH₂ONa / Heating

7: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

8: dimethylformamide / 2 h / Heating

With potassium hydroxide; thionyl chloride; hydrogen; tin(IV) chloride; sodium phenyl-methanolate; diborane; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

[1,4-phenylene]-bis(3-hydroxypropane) (19417-58-4) → C26H36N2 (144582-02-5)

Guidance literature:

Multi-step reaction with 9 steps

1: HBr

2: ethanol

3: aq. KOH

4: SOCl₂ / 0.5 h / Heating

5: 57 percent / SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

6: 80 percent / B₂H₆ / tetrahydrofuran

7: 86 percent / PhCH₂ONa / Heating

8: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

9: dimethylformamide / 2 h / Heating

With potassium hydroxide; thionyl chloride; hydrogen bromide; hydrogen; tin(IV) chloride; sodium phenyl-methanolate; diborane; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

3,3'-(1,4-phenylene)dipropanoic acid (4251-21-2) → C26H36N2 (144582-02-5)

Guidance literature:

Multi-step reaction with 11 steps

1: 1) SOCl₂, 2) NEt₃

2: B₂H₆

3: HBr

4: ethanol

5: aq. KOH

6: SOCl₂ / 0.5 h / Heating

7: 57 percent / SnCl₄ / CH₂Cl₂; nitromethane / Ambient temperature

8: 80 percent / B₂H₆ / tetrahydrofuran

9: 86 percent / PhCH₂ONa / Heating

10: H₂ / 10percent Pd/C / tetrahydrofuran / 760 Torr

11: dimethylformamide / 2 h / Heating

With potassium hydroxide; thionyl chloride; hydrogen bromide; hydrogen; tin(IV) chloride; triethylamine; sodium phenyl-methanolate; diborane; palladium on activated charcoal; In tetrahydrofuran; nitromethane; ethanol; dichloromethane; N,N-dimethyl-formamide;

upstream raw materials:

C₂₈H₃₆N₂O₄

[1,4-phenylene]-bis(3-hydroxypropane)

1,4-bis-(3-bromopropyl)-benzene

3,3'-(1,4-phenylene)dipropanoic acid

Downstream raw materials:

1,4-Bis<4-(5-formyl-2,4-dimethylpyrrol-3-yl)butyl>benzene

1,4-Bis<4-<5-(2-cyano-2-methoxycarbonylvinyl)-2,4-dimethylpyrrol-3-yl>butyl>benzene

(E)-3-{5-Chloromethyl-4-[4-(4-{4-[2-chloromethyl-5-((E)-2-cyano-2-methoxycarbonyl-vinyl)-4-methyl-1H-pyrrol-3-yl]-butyl}-phenyl)-butyl]-3-methyl-1H-pyrrol-2-yl}-2-cyano-acrylic acid methyl ester

1,4-Bis<4-<2-((5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl)-5-formyl-4-methylpyrrol-3-yl>butyl>benzene