(2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate

Base Information

Chemical Name:(2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate
CAS No.:1374767-37-9
Molecular Formula:C₂₃H₃₁ClO₅
Molecular Weight:422.949
Hs Code.:

Synonyms:(2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate

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Chemical Property of (2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate

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Technology Process of (2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate

There total 9 articles about (2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1374768-06-5
C₁₅H₂₅BrO₂

: 83324-59-8
3-chloro-4,6-dihydroxy-2-methyl-benzaldehyde

: 1374767-37-9
(2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate

Guidance literature:: With calcium(II) chloride dihydrate; potassium hydroxide; In methanol; at 0 - 20 ℃; for 14h;

Reference yield:

: C₁₅H₂₅BrO₂

: 83324-59-8
3-chloro-4,6-dihydroxy-2-methyl-benzaldehyde

: 1374767-37-9
(2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate

Guidance literature:: With calcium(II) chloride dihydrate; potassium hydroxide; In methanol; at 0 - 20 ℃; for 14h;

Reference yield:

: 3282-30-2
pivaloyl chloride

: 1374767-37-9
(2E,6E)-8-(3-chloro-5-formyl-2,6-dihydroxy-4-methylphenyl)-3,6-dimethyl-2,6-octadienyl pivalate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine; dmap / chloroform / 12 h / 0 - 20 °C

2: carbon tetrabromide; TOP / diethyl ether / 2 h / 0 °C

3: calcium(II) chloride dihydrate; potassium hydroxide / methanol / 14 h / 0 - 20 °C

With dmap; calcium(II) chloride dihydrate; carbon tetrabromide; TOP; triethylamine; potassium hydroxide; In methanol; diethyl ether; chloroform;