dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl}

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Chemical Name:dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl}
CAS No.:98088-32-5
Molecular Formula:C₃₀H₄₄O₂P₂Ru
Molecular Weight:599.696
Hs Code.:

Synonyms:dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl}

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Chemical Property of dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl}

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Technology Process of dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl}

There total 1 articles about dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.5%

: (η(5)-C5Me5)(CO)2Ru(P(SiMe3)2)

: 79074-00-3
2,4,6-tri-t-butylphenylphosphonous dichloride

: 98088-32-5
dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl}

Guidance literature:: In tetrahydrofuran; byproducts: (CH3)3SiCl; addn. of solid dichlorophosphane to Ru complex soln. at 0°C; stirring at 20°C, 30 min; evapn. to dryness; taking residue into hexane; filtration; washing residue with hexane; drying (vac.); pptn. from THF/pentane;

Reference yield: 21.0%

: 98088-32-5
dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium{(2,4,6-tri-tert-butylphenyl)diphosphenyl}

: 33462-81-6
{c-C₃H₅SPh₂}BF₄

: 112713-08-3
{dicarbonyl(η5-pentamethylcyclopentadienyl)ruthenium}PC(CH2CH2)P(2,4,6-tri-tert-butylphenyl)

: 139-66-2
diphenyl sulfide

Guidance literature:: With KO-t-Bu; In tetrahydrofuran; addn. of KO-t-Bu in THF to the Fe compd. and P compd. in THF (inert atmosphere); filtn., evapn. (vacuum), soln. in petroleum ether, concn. and standing at -28°C; elem. anal.;