2,4,6-tri-t-butylphenylphosphonous dichloride

Base Information

Chemical Name:2,4,6-tri-t-butylphenylphosphonous dichloride
CAS No.:79074-00-3
Molecular Formula:C₁₈H₂₉Cl₂P
Molecular Weight:347.308
Hs Code.:

Synonyms:2,4,6-tri-t-butylphenylphosphonous dichloride

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Chemical Property of 2,4,6-tri-t-butylphenylphosphonous dichloride

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Technology Process of 2,4,6-tri-t-butylphenylphosphonous dichloride

There total 8 articles about 2,4,6-tri-t-butylphenylphosphonous dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 3975-77-7
1-bromo-2,4,6-tri-tert-butylbenzene

: 79074-00-3
2,4,6-tri-t-butylphenylphosphonous dichloride

Guidance literature:: 1-bromo-2,4,6-tri-tert-butylbenzene; With magnesium; In tetrahydrofuran; for 1h; Inert atmosphere; Schlenk technique; Reflux;

With 1,4-dioxane; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere; Schlenk technique;

With phosphorus trichloride; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1002/chem.201806334

Reference yield:

: 83466-54-0,93602-74-5,79073-99-7
Bis(2,4,6-tri-tert-butylphenyl)diphosphen

: 79074-00-3
2,4,6-tri-t-butylphenylphosphonous dichloride

Guidance literature:: With chlorine; In tetrachloromethane; Ambient temperature;
DOI:10.1021/ja00405a054

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 83115-12-2
(2,4,6-tri-tert-butylphenyl)phosphine

: 79074-00-3
2,4,6-tri-t-butylphenylphosphonous dichloride

Guidance literature:: (2,4,6-tri-tert-butylphenyl)phosphine; With n-butyllithium; In tetrahydrofuran; at -80 ℃; for 0.5h; Inert atmosphere;

chloro-trimethyl-silane; In tetrahydrofuran; Inert atmosphere;
DOI:10.1039/c5dt02757h