ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate

Base Information

Chemical Name:ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate
CAS No.:753025-13-7
Molecular Formula:C₁₆H₁₇N₃O₅S
Molecular Weight:363.394
Hs Code.:

Synonyms:ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate

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Chemical Property of ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate

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Technology Process of ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate

There total 5 articles about ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.7%

: 98-68-0
4-methoxy-phenyl-sulphonyl chloride

: 238749-51-4
ethyl 1-methyl-1,4-dihydropyrrolo[2,3-d]imidazole-5-carboxylate

: 753025-13-7
ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate

Guidance literature:: With acetic acid; In chloroform; for 3h; Heating;
DOI:10.1016/S0040-4020(03)00138-8

Reference yield:

: 39021-62-0
1-methylimidazole-5-carbaldehyde

: 753025-13-7
ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 73 percent / Na / ethanol / 2 h / -10 °C

2.1: 39 percent / xylene / 2 h / Heating

3.1: t-BuLi / tetrahydrofuran / 0.25 h / -78 °C

3.2: 63 percent / tetrahydrofuran; benzene / -10 - 25 °C

With tert.-butyl lithium; sodium; In tetrahydrofuran; ethanol; xylene;

Reference yield:

: 38993-84-9
(1-methyl-1H-imidazol-5-yl)methanol

: 753025-13-7
ethyl-1-methyl-4-(4-methoxy benzenesulfonyl)pyrrolo[2,3-d]imidazole-5-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 95 percent / MnO₂ / CHCl₃ / 12 h / Heating

2.1: 73 percent / Na / ethanol / 2 h / -10 °C

3.1: 39 percent / xylene / 2 h / Heating

4.1: t-BuLi / tetrahydrofuran / 0.25 h / -78 °C

4.2: 63 percent / tetrahydrofuran; benzene / -10 - 25 °C

With manganese(IV) oxide; tert.-butyl lithium; sodium; In tetrahydrofuran; ethanol; chloroform; xylene;