C₂₇H₃₁F₃N₂O₅

Base Information

Chemical Name:C₂₇H₃₁F₃N₂O₅
CAS No.:860797-25-7
Molecular Formula:C₂₇H₃₁F₃N₂O₅
Molecular Weight:520.549
Hs Code.:

C<sub>27</sub>H<sub>31</sub>F<sub>3</sub>N<sub>2</sub>O<sub>5</sub>

Synonyms:C₂₇H₃₁F₃N₂O₅

Suppliers and Price of C₂₇H₃₁F₃N₂O₅

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₇H₃₁F₃N₂O₅

Chemical Property:

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Technology Process of C₂₇H₃₁F₃N₂O₅

There total 15 articles about C₂₇H₃₁F₃N₂O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₃F₃N₂O₅*ClH

: 860797-25-7
C₂₇H₃₁F₃N₂O₅

Guidance literature:: With methanol; lithium hydroxide; water; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 693248-12-3
2-tert-butoxy-5-trifluoromethylbenzonitrile

: 860797-25-7
C₂₇H₃₁F₃N₂O₅

Guidance literature:: Multi-step reaction with 8 steps

1: ammonia; hydrogen / Raney 2800 nickel / ethanol; water / 24 h / 2585.81 Torr

2: dmap; 1,2-dichloro-ethane / dichloromethane / 72 h / 20 °C

3: hydrogenchloride / 1,4-dioxane / 3.5 h / 20 °C

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 20 °C

5: formaldehyd; toluene-4-sulfonic acid / benzene / 4 h / Heating / reflux

6: potassium carbonate / methanol; water / 4.5 h / 20 - 50 °C

7: sodium tris(acetoxy)borohydride / dichloromethane / 12 h / 20 °C / Molecular sieve 4A

8: methanol; lithium hydroxide; water / tetrahydrofuran / 20 °C

With hydrogenchloride; methanol; dmap; lithium hydroxide; formaldehyd; sodium tris(acetoxy)borohydride; ammonia; water; hydrogen; potassium carbonate; toluene-4-sulfonic acid; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; Raney 2800 nickel; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; benzene;

Reference yield:

: 4088-84-0
2-fluoro-5-trifluoromethyl-benzonitrile

: 860797-25-7
C₂₇H₃₁F₃N₂O₅

Guidance literature:: Multi-step reaction with 9 steps

1: tetrahydrofuran / 0 - 20 °C

2: ammonia; hydrogen / Raney 2800 nickel / ethanol; water / 24 h / 2585.81 Torr

3: dmap; 1,2-dichloro-ethane / dichloromethane / 72 h / 20 °C

4: hydrogenchloride / 1,4-dioxane / 3.5 h / 20 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 2.5 h / 20 °C

6: formaldehyd; toluene-4-sulfonic acid / benzene / 4 h / Heating / reflux

7: potassium carbonate / methanol; water / 4.5 h / 20 - 50 °C

8: sodium tris(acetoxy)borohydride / dichloromethane / 12 h / 20 °C / Molecular sieve 4A

9: methanol; lithium hydroxide; water / tetrahydrofuran / 20 °C

With hydrogenchloride; methanol; dmap; lithium hydroxide; formaldehyd; sodium tris(acetoxy)borohydride; ammonia; water; hydrogen; potassium carbonate; toluene-4-sulfonic acid; 1,2-dichloro-ethane; N-ethyl-N,N-diisopropylamine; Raney 2800 nickel; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; water; benzene;