cis-23-(dioxolan-2-yl)tricos-12-enyltriphenylphosphonium bromide

Base Information

Chemical Name:cis-23-(dioxolan-2-yl)tricos-12-enyltriphenylphosphonium bromide
CAS No.:113309-15-2
Molecular Formula:Br*C₄₄H₆₄O₂P
Molecular Weight:735.869
Hs Code.:

Synonyms:cis-23-(dioxolan-2-yl)tricos-12-enyltriphenylphosphonium bromide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of cis-23-(dioxolan-2-yl)tricos-12-enyltriphenylphosphonium bromide

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Technology Process of cis-23-(dioxolan-2-yl)tricos-12-enyltriphenylphosphonium bromide

There total 13 articles about cis-23-(dioxolan-2-yl)tricos-12-enyltriphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 110843-42-0
cis,trans-24-bromotetracos-12-enal ethylene acetal

: 603-35-0
triphenylphosphine

: 113309-15-2,113309-16-3
23-(Dioxolan-2-yl)tricos-12-enyl(triphenyl)phosphonium bromide

Guidance literature:: With trimethyl orthoformate; In acetonitrile; for 60h; Heating;
DOI:10.1039/P19870002447

Reference yield:

: 84451-53-6
cis-24-bromotetracos-12-enal ethylene acetal

: 603-35-0
triphenylphosphine

: 1779-49-3
Methyltriphenylphosphonium bromide

: 113309-15-2
cis-23-(dioxolan-2-yl)tricos-12-enyltriphenylphosphonium bromide

Guidance literature:: With trimethyl orthoformate;

Reference yield:

: 84451-51-4
12-bromododecanal ethylene acetal

: 113309-15-2,113309-16-3
23-(Dioxolan-2-yl)tricos-12-enyl(triphenyl)phosphonium bromide

Guidance literature:: Multi-step reaction with 4 steps

1: 2,2-dimethyl-1,3-dioxolane / acetonitrile / 72 h / Heating

2: LDA / tetrahydrofuran / 0.5 h / -10 °C

3: tetrahydrofuran / 16 h / Ambient temperature

4: 2,2-dimethyl-1,3-dioxolane / acetonitrile / 66 h

With 2,2-dimethyl-1,3-dioxolane; lithium diisopropyl amide; In tetrahydrofuran; acetonitrile;
DOI:10.1039/p19960001635