C₃₄H₆₀N₂O₆Si₃

Base Information

• Chemical Name: C₃₄H₆₀N₂O₆Si₃
• CAS No.: 1613530-21-4
• Molecular Formula: C₃₄H₆₀N₂O₆Si₃
• Molecular Weight: 677.117
• Mol file: 1613530-21-4.mol

Synonyms:C₃₄H₆₀N₂O₆Si₃

Chemical Property of C₃₄H₆₀N₂O₆Si₃

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₄H₆₀N₂O₆Si₃

There total 2 articles about C₃₄H₆₀N₂O₆Si₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

tert-butyldimethylsilyl chloride (18162-48-6) → C34H60N2O6Si3 (1613530-21-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 30 °C

2.1: N,O-bis-(trimethylsilyl)-acetamide / dichloromethane / 4 h / 40 °C

2.2: 120 h / Reflux

With 1H-imidazole; N,O-bis-(trimethylsilyl)-acetamide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

pseudouridine (1445-07-4) → C34H60N2O6Si3 (1613530-21-4)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 1H-imidazole / N,N-dimethyl-formamide / 30 °C

2.1: N,O-bis-(trimethylsilyl)-acetamide / dichloromethane / 4 h / 40 °C

2.2: 120 h / Reflux

With 1H-imidazole; N,O-bis-(trimethylsilyl)-acetamide; In dichloromethane; N,N-dimethyl-formamide;

Reference yield: 51.0%

C34H60N2O6Si3 (1613530-21-4) → 1-benzyl-pseudouridine (1613530-22-5)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;

upstream raw materials:

pseudouridine

tert-butyldimethylsilyl chloride

Downstream raw materials:

1-benzyl-pseudouridine

Refernces

• 1、 -. "ALTERNATIVE NUCLEIC ACID MOLECULES AND USES THEREOF". . . Retrieved 2016/06/28.
• 2、 -. "MODIFIED NUCLEIC ACID MOLECULES AND USES THEREOF". . . Retrieved 2014/07/07.