p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

Base Information

Chemical Name:p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside
CAS No.:1316822-81-7
Molecular Formula:C₃₀H₄₆N₄O₁₆
Molecular Weight:718.712
Hs Code.:

p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

Synonyms:p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

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Chemical Property of p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

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Technology Process of p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

There total 13 articles about p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1144040-11-8
p-nitrophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

: 1316822-81-7
p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

Guidance literature:: With 10% palladium on activated charcoal; hydrogen; In water; for 1h;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 1147438-51-4
p-nitrophenyl 3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranoside

: 1316822-81-7
p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

1.2: Dowex H+

2.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; acetonitrile / 1 h / 20 °C

3.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

3.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

4.1: water; acetic acid / dichloromethane / 48 h / 20 °C

5.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

5.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

6.1: sodium methylate / methanol / 0.33 h / 20 °C

6.2: Dowex H+

7.1: hydrazine / ethanol / 70 °C

8.1: dmap / pyridine / 2 h / 20 °C

9.1: pyridine / 20 °C

10.1: sodium methylate / methanol / 0.5 h

10.2: 1 h

10.3: Dowex H+

11.1: 10% palladium on activated charcoal; hydrogen / water / 1 h

With dmap; N-iodo-succinimide; 10% palladium on activated charcoal; water; hydrogen; sodium methylate; toluene-4-sulfonic acid; acetic acid; hydrazine; In pyridine; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2011.03.036

Reference yield:

: 100-02-7,78813-13-5,89830-32-0
4-nitro-phenol

: 1316822-81-7
p-aminophenyl 2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->3)-2-acetamido-2-deoxy-β-D-glucopyranosyl-(1->6)-2-acetamido-2-deoxy-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 12 steps

1.1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / -20 °C

2.1: sodium methylate / methanol / 0.5 h / 20 °C / pH 10

2.2: Dowex H+

3.1: toluene-4-sulfonic acid / N,N-dimethyl-formamide; acetonitrile / 1 h / 20 °C

4.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

4.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

5.1: water; acetic acid / dichloromethane / 48 h / 20 °C

6.1: N-iodo-succinimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere; Molecular sieve

6.2: 1 h / -30 °C / Inert atmosphere; Molecular sieve

7.1: sodium methylate / methanol / 0.33 h / 20 °C

7.2: Dowex H+

8.1: hydrazine / ethanol / 70 °C

9.1: dmap / pyridine / 2 h / 20 °C

10.1: pyridine / 20 °C

11.1: sodium methylate / methanol / 0.5 h

11.2: 1 h

11.3: Dowex H+

12.1: 10% palladium on activated charcoal; hydrogen / water / 1 h

With dmap; N-iodo-succinimide; trimethylsilyl trifluoromethanesulfonate; 10% palladium on activated charcoal; water; hydrogen; sodium methylate; toluene-4-sulfonic acid; acetic acid; hydrazine; In pyridine; methanol; ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.carres.2011.03.036