1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol

Base Information

• Chemical Name: 1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol
• CAS No.: 101639-66-1
• Molecular Formula: C₂₅H₃₄N₄O₃
• Molecular Weight: 438.57

Synonyms:1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol

Chemical Property of 1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol

Chemical Property:

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Technology Process of 1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol

There total 2 articles about 1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

1-[2-(cyclopropyl-methoxy)-ethyl]-4-(2,3-epoxypropoxy)-benzene (63659-17-6) + 1-(p-azidophenyl)-2-methyl-2-propylamine (101639-65-0) → 1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol (101639-66-1)

Guidance literature:

In ethanol; for 6h; Heating;

DOI:10.1002/jps.2600741024

Reference yield:

4-(β-amino-isobutyl)-aniline (51131-55-6) → 1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol (101639-66-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 96 percent / 2M HCl, NaNO₂, NaN₃ / H₂O / 0.25 h

2: 60 percent / ethanol / 6 h / Heating

With hydrogenchloride; sodium azide; sodium nitrite; In ethanol; water;

DOI:10.1002/jps.2600741024

Reference yield: 98.0%

1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(azidophenyl)-2-methyl-2-propylamine>-2-propanol (101639-66-1) → 1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(aminophenyl)-2-methyl-2-propylamine>-2-propanol (101639-67-2)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 0.25h; Ambient temperature;

DOI:10.1002/jps.2600741024

upstream raw materials:

1-[2-(cyclopropyl-methoxy)-ethyl]-4-(2,3-epoxypropoxy)-benzene

1-(p-azidophenyl)-2-methyl-2-propylamine

4-(β-amino-isobutyl)-aniline

Downstream raw materials:

1-<4-(2-cyclopropylmethoxyethyl)phenoxy>-3-<1-p-(aminophenyl)-2-methyl-2-propylamine>-2-propanol

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