C₁₇H₂₁BrFN₃O₂

Base Information

Chemical Name:C₁₇H₂₁BrFN₃O₂
CAS No.:1374001-21-4
Molecular Formula:C₁₇H₂₁BrFN₃O₂
Molecular Weight:398.275
Hs Code.:

C<sub>17</sub>H<sub>21</sub>BrFN<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₇H₂₁BrFN₃O₂

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Chemical Property of C₁₇H₂₁BrFN₃O₂

Chemical Property:

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Technology Process of C₁₇H₂₁BrFN₃O₂

There total 8 articles about C₁₇H₂₁BrFN₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 131543-46-9,107-22-2
Glyoxal

: 1374001-20-3
tert-butyl [(2S)-2-(5-bromo-2-fluorophenyl)-4-oxobutan-2-yl]carbamate

: 1374001-21-4
C₁₇H₂₁BrFN₃O₂

Guidance literature:: With ammonium bicarbonate; In methanol; water; at 20 ℃; for 24h;

Reference yield:

: 93777-26-5
5-bromo-2-fluorobenzaldehyde

: 1374001-21-4
C₁₇H₂₁BrFN₃O₂

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 1 h / -78 - -5 °C / Inert atmosphere

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 7 h / Reflux

3.1: titanium(IV) tetraethanolate / tetrahydrofuran / 4.5 h / Inert atmosphere; Reflux

4.1: diethyl ether / 3 h / -78 - 0 °C / Inert atmosphere

5.1: hydrogenchloride / methanol; 1,4-dioxane / 1 h / 20 °C

6.1: tetrahydrofuran / 8 h / 60 °C

7.1: ozone / dichloromethane / -78 °C

7.2: 1 h / -78 - 20 °C / Inert atmosphere

8.1: ammonium bicarbonate / methanol; water / 24 h / 20 °C

With hydrogenchloride; titanium(IV) tetraethanolate; ammonium bicarbonate; ozone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; ethyl acetate;

Reference yield:

: 552331-15-4
1-(5-bromo-2-fluorophenyl)ethan-1-ol

: 1374001-21-4
C₁₇H₂₁BrFN₃O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 7 h / Reflux

2.1: titanium(IV) tetraethanolate / tetrahydrofuran / 4.5 h / Inert atmosphere; Reflux

3.1: diethyl ether / 3 h / -78 - 0 °C / Inert atmosphere

4.1: hydrogenchloride / methanol; 1,4-dioxane / 1 h / 20 °C

5.1: tetrahydrofuran / 8 h / 60 °C

6.1: ozone / dichloromethane / -78 °C

6.2: 1 h / -78 - 20 °C / Inert atmosphere

7.1: ammonium bicarbonate / methanol; water / 24 h / 20 °C

With hydrogenchloride; titanium(IV) tetraethanolate; ammonium bicarbonate; ozone; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1,4-dioxane; methanol; diethyl ether; dichloromethane; water; ethyl acetate;