N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane

Base Information

Chemical Name:N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane
CAS No.:357383-37-0
Molecular Formula:C₂₆H₃₉BrN₂O₄S₂
Molecular Weight:587.643
Hs Code.:

Synonyms:N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane

Chemical Property:

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Technology Process of N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane

There total 3 articles about N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 109-64-8
1,3-dibromo-propane

: 206991-72-2
N,N'-bis(mesitylenesulfonyl)-N-ethyl-1,3-diaminopropane

: 357383-37-0
N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane

Guidance literature:: N,N'-bis(mesitylenesulfonyl)-N-ethyl-1,3-diaminopropane; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

1,3-dibromo-propane; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Further stages.;
DOI:10.1021/jm000532q

Reference yield:

: 773-64-8
2-mesitylenesulphonyl chloride

: 357383-37-0
N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 88 percent / aq. NaOH / CH₂Cl₂ / 18 h / 20 °C

2.1: NaH / dimethylformamide / 0.5 h / 20 °C

2.2: 71 percent / dimethylformamide / 18 h / 20 °C

With sodium hydroxide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm000532q

Reference yield:

: 10563-23-2
N-ethyl-1,3-diaminopropane

: 357383-37-0
N,N'-bis(mesitylenesulfonyl)-N-(3-bromopropyl)-N'-ethyl-1,3-diaminopropane

Guidance literature:: Multi-step reaction with 2 steps

1.1: 88 percent / aq. NaOH / CH₂Cl₂ / 18 h / 20 °C

2.1: NaH / dimethylformamide / 0.5 h / 20 °C

2.2: 71 percent / dimethylformamide / 18 h / 20 °C

With sodium hydroxide; sodium hydride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm000532q