O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose

Base Information

Chemical Name:O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose
CAS No.:868992-03-4
Molecular Formula:C₂₃H₃₀O₁₁
Molecular Weight:482.485
Hs Code.:

Synonyms:O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose

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Technology Process of O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose

There total 3 articles about O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 868992-17-0
O-[3-(4-phenylmethoxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galacto-pyranose

: 868992-03-4
O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; at 20 ℃; for 2h; under 760 Torr;
DOI:10.1016/j.tet.2005.08.018

Reference yield:

: 61440-45-7
3-[4-(benzyloxy)phenyl]propan-1-ol

: 868992-03-4
O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / trimethylsilyl triflate / CH₂Cl₂ / 2 h / 0 °C

2: 99 percent / hydrogen / Pd/C / ethanol / 2 h / 20 °C / 760 Torr

With trimethylsilyl trifluoromethanesulfonate; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2005.08.018

Reference yield:

: 74808-10-9,86520-63-0,87119-53-7,92052-29-4,121238-27-5,142831-80-9,127061-80-7
2,3,4,6-tetra-O-acetyl-D-galactopyranosyl trichloroacetimidate

: 868992-03-4
O-[3-(4-hydroxyphenyl)-1-propyl]-(2,3,4,6-O-tetraacetyl)-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 33 percent / trimethylsilyl triflate / CH₂Cl₂ / 2 h / 0 °C

2: 99 percent / hydrogen / Pd/C / ethanol / 2 h / 20 °C / 760 Torr

With trimethylsilyl trifluoromethanesulfonate; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/j.tet.2005.08.018