2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide

Base Information

Chemical Name:2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide
CAS No.:1410037-07-8
Molecular Formula:C₁₂H₁₅F₂NO₃Se
Molecular Weight:338.213
Hs Code.:

Synonyms:2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide

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Technology Process of 2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide

There total 2 articles about 2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1410037-04-5
C₁₂H₁₄F₂O₃Se

: 6638-79-5
N,O-dimethylhydroxylamine*hydrochloride

: 1410037-07-8
2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide

Guidance literature:: N,O-dimethylhydroxylamine*hydrochloride; With n-butyllithium; In tetrahydrofuran; hexane; at -80 - 20 ℃; for 0.0833333h;

C₁₂H₁₄F₂O₃Se; In tetrahydrofuran; hexane; at -80 ℃; for 1h;
DOI:10.1039/c2cc35876j

Reference yield:

: 71338-48-2
phenylselanylacetaldehyde

: 1410037-07-8
2,2-difluoro-3-hydroxy-N-methoxy-N-methyl-4-phenylselenenyl butyramide

Guidance literature:: Multi-step reaction with 2 steps

1.1: zinc; acetic acid; copper diacetate / 0.08 h / 80 - 110 °C / Reflux

1.2: 1 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.08 h / -80 - 20 °C

2.2: 1 h / -80 °C

With n-butyllithium; copper diacetate; acetic acid; zinc; In tetrahydrofuran; hexane;
DOI:10.1039/c2cc35876j