C₂₈H₃₇IO₂

Base Information

Chemical Name:C₂₈H₃₇IO₂
CAS No.:1256563-88-8
Molecular Formula:C₂₈H₃₇IO₂
Molecular Weight:532.505
Hs Code.:

C<sub>28</sub>H<sub>37</sub>IO<sub>2</sub>

Synonyms:C₂₈H₃₇IO₂

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Chemical Property of C₂₈H₃₇IO₂

Chemical Property:

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Technology Process of C₂₈H₃₇IO₂

There total 7 articles about C₂₈H₃₇IO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1256563-87-7
C₂₇H₃₅IO₃

: 1779-49-3
Methyltriphenylphosphonium bromide

: 1256563-88-8
C₂₈H₃₇IO₂

Guidance literature:: Methyltriphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;

C₂₇H₃₅IO₃; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol102398y

Reference yield:

: 1256563-86-6
2,5-bishexyloxy-4-iodostyrene

: 1256563-88-8
C₂₈H₃₇IO₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform; benzene / 40 h / Inert atmosphere; Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2.2: 0 - 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; potassium tert-butylate; In tetrahydrofuran; chloroform; benzene; 2.1: Wittig reaction / 2.2: Wittig reaction;
DOI:10.1021/ol102398y

Reference yield:

: 111-25-1
1-bromo-hexane

: 1256563-88-8
C₂₈H₃₇IO₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydrosulfite pentahydrate; tetrabutylammomium bromide; potassium hydroxide / water; toluene / Cooling with ice; Reflux

2.1: Iodine monochloride / methanol / Cooling with ice; Reflux

3.1: n-butyllithium / diethyl ether; hexane / 0.75 h / 0 °C / Inert atmosphere

3.2: 2 h / 20 °C / Inert atmosphere

4.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / chloroform; benzene / 40 h / Inert atmosphere; Reflux

6.1: potassium tert-butylate / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

6.2: 0 - 20 °C / Inert atmosphere

With tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; n-butyllithium; sodium hydrosulfite pentahydrate; potassium tert-butylate; tetrabutylammomium bromide; Iodine monochloride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; hexane; chloroform; water; toluene; benzene; 4.1: Wittig reaction / 6.1: Wittig reaction / 6.2: Wittig reaction;
DOI:10.1021/ol102398y