3-bromo-N-cyclohexylbenzamide

Base Information

Chemical Name:3-bromo-N-cyclohexylbenzamide
CAS No.:59507-55-0
Molecular Formula:C13H16BrNO
Molecular Weight:282.18
Hs Code.:2924299090
DSSTox Substance ID:DTXSID20367960
Nikkaji Number:J2.409.920B
Wikidata:Q82154181
Mol file:59507-55-0.mol

Synonyms:3-bromo-N-cyclohexylbenzamide;59507-55-0;N-Cyclohexyl 3-bromobenzamide;N-Cyclohexyl3-bromobenzamide;Oprea1_163420;N-Cyclohexyl-3-bromobenzamide;SCHEMBL613993;DTXSID20367960;VRUMXGVWUFXLAH-UHFFFAOYSA-N;MFCD00554081;AKOS000178267;BS-23734;CS-0213502

Suppliers and Price of 3-bromo-N-cyclohexylbenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
N-Cyclohexyl3-bromobenzamide
1g
$ 175.00

SynQuest Laboratories
3-Bromo-N-cyclohexylbenzamide
5 g
$ 520.00

SynQuest Laboratories
3-Bromo-N-cyclohexylbenzamide
1 g
$ 144.00

Crysdot
3-Bromo-N-cyclohexylbenzamide 95+%
10g
$ 417.00

Chemenu
3-Bromo-N-cyclohexylbenzamide 95%
10g
$ 394.00

Apolloscientific
3-Bromo-N-cyclohexylbenzamide
1g
$ 131.00

Apolloscientific
3-Bromo-N-cyclohexylbenzamide
5g
$ 472.00

American Custom Chemicals Corporation
3-BROMO-N-CYCLOHEXYL BENZAMIDE 95.00%
1G
$ 708.48

American Custom Chemicals Corporation
3-BROMO-N-CYCLOHEXYL BENZAMIDE 95.00%
5G
$ 1223.72

AK Scientific
N-Cyclohexyl3-bromobenzamide
25g
$ 900.00

Total 10 raw suppliers

Chemical Property of 3-bromo-N-cyclohexylbenzamide

Chemical Property:

Vapor Pressure:1.12E-06mmHg at 25°C
Melting Point:166-168°C
Refractive Index:1.584
Boiling Point:402.1°C at 760 mmHg
PKA:14.44±0.20(Predicted)
Flash Point:197°C
PSA：29.10000
Density:1.37g/cm³
LogP:3.90250
Storage Temp.:Keep Cold
XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:281.04153
Heavy Atom Count:16
Complexity:238

Purity/Quality:

97% ^*data from raw suppliers

N-Cyclohexyl3-bromobenzamide ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)NC(=O)C2=CC(=CC=C2)Br

Technology Process of 3-bromo-N-cyclohexylbenzamide

There total 4 articles about 3-bromo-N-cyclohexylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1711-09-7
3-bromobenzoyl chloride

: 108-91-8,157973-60-9
cyclohexylamine

: 59507-55-0
3-bromo-N-cyclohexylbenzamide

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 76.0%

: 13144-62-2
2-(cyclohexylamino)-2-oxoacetic acid

: potassium (3-bromophenyl)trifluoroborate

: 59507-55-0
3-bromo-N-cyclohexylbenzamide

Guidance literature:: With dipotassium peroxodisulfate; palladium diacetate; silver nitrate; In water; dimethyl sulfoxide; acetonitrile; at 70 ℃; for 0.166667h;
DOI:10.1039/c1cc11635e

Reference yield: 61.0%

: 3132-99-8
m-bromobenzoic aldehyde

: 108-91-8,157973-60-9
cyclohexylamine

: 59507-55-0
3-bromo-N-cyclohexylbenzamide

Guidance literature:: m-bromobenzoic aldehyde; With ethyl tribromoacetate; dibenzoyl peroxide; In chlorobenzene; at 110 ℃; for 24h;

cyclohexylamine; With triethylamine; In chlorobenzene; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2006.11.013