trans-cyclohexane-1,2-diyl dibenzoate

Base Information

• Chemical Name: trans-cyclohexane-1,2-diyl dibenzoate
• CAS No.: 53226-58-7
• Molecular Formula: C₂₀H₂₀O₄
• Molecular Weight: 324.376
• Mol file: 53226-58-7.mol

Synonyms:trans-cyclohexane-1,2-diyl dibenzoate

Chemical Property of trans-cyclohexane-1,2-diyl dibenzoate

Chemical Property:

Purity/Quality:

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Technology Process of trans-cyclohexane-1,2-diyl dibenzoate

There total 16 articles about trans-cyclohexane-1,2-diyl dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

trans-1,2-cyclohexandiol (1460-57-7) + benzoyl chloride (98-88-4) → trans-cyclohexane-1,2-diyl dibenzoate (53226-58-7)

Guidance literature:

With N,N,N,N,-tetramethylethylenediamine; 4 A molecular sieve; In dichloromethane; at -78 ℃; for 0.333333h;

DOI:10.1055/s-1999-3521

Reference yield: 93.0%

trans-1,2-cyclohexandiol (1460-57-7) + N-benzoyl-4-(N,N-dimethylamino)pyridinium chloride (64548-92-1) → trans-cyclohexane-1,2-diyl dibenzoate (53226-58-7)

Guidance literature:

With triethylamine; In dichloromethane; for 2h;

DOI:10.1080/00397919708005004

Reference yield: 88.0%

trans-1,2-Bis(thiobenzoyloxy)cyclohexan (57701-19-6,79239-72-8) → trans-cyclohexane-1,2-diyl dibenzoate (53226-58-7)

Guidance literature:

With benzeneseleninic anhydride; In tetrahydrofuran; for 2h; Ambient temperature;

upstream raw materials:

cyclohexane

silver benzoate

(+/-)-trans-4,5-bis-benzoyloxy-cyclohexene

cyclohexane-1,2-epoxide