[Cl₂NN]Cu-NHAd

Base Information

• Chemical Name: [Cl₂NN]Cu-NHAd
• CAS No.: 1215209-26-9
• Molecular Formula: C₂₇H₂₉Cl₄CuN₃
• Molecular Weight: 600.905

Synonyms:[Cl₂NN]Cu-NHAd

Chemical Property of [Cl₂NN]Cu-NHAd

Chemical Property:

Purity/Quality:

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Technology Process of [Cl₂NN]Cu-NHAd

There total 2 articles about [Cl₂NN]Cu-NHAd which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

[(Cu(CH(C(CH3)NC6H3Cl2)2))2(μ-Cl)2] (1261138-80-0) + lithium adamant-1-ylamide (68295-36-3) → [Cl2NN]Cu-NHAd (1215209-26-9)

Guidance literature:

In diethyl ether; byproducts: LiCl; at -35°C; isolated from pentane;

DOI:10.1002/anie.201003676

Reference yield:

[Cl2NN]Cu-OtBu (1215209-38-3) + 1-Adamantanamine (768-94-5) → [Cl2NN]Cu-NHAd (1215209-26-9)

Guidance literature:

In benzene; not isolated, detected by UV/Vis;

DOI:10.1002/anie.201003676

Reference yield: 87.0%

ethylbenzene (100-41-4,27536-89-6) + [Cl2NN]Cu-NHAd (1215209-26-9) → N-(1-phenylethyl)-1-aminoadamantane (1034159-49-3) + 1-Adamantanamine (768-94-5)

Guidance literature:

In n-heptane; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.201003676

upstream raw materials:

[(Cu(CH(C(CH3)NC6H3Cl2)2))2(μ-Cl)2]

lithium adamant-1-ylamide

[Cl₂NN]Cu-OtBu

1-Adamantanamine

Downstream raw materials:

N-(1-adamantyl)imidoethane

1-Adamantanamine

N-(1-phenylethyl)-1-aminoadamantane

AdNHC(CD₃)(C₆D₅)

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